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Coordination compounds are a significant part of inorganic chemistry. Experiments often involve the synthesis and characterization of these compounds, which have applications in catalysis, drug delivery, and more.
The synthesis typically involves the reaction of PhPCl(_2) with a source of Se(^2-) ions under an inert atmosphere (nitrogen or argon).
Inorganic Experiments , edited by J. Derek Woollins , is a standard laboratory manual for inorganic chemistry, featuring contributions from various international experts. It is structured into three difficulty levels— introductory, intermediate, and advanced Inorganic Experiments Woollins.pdf
The synthesis relies on the oxidation of Iron(II) to Iron(III). The intermediate ferrous oxalate is insoluble, which allows for its purification before the coordination step. The hydrogen peroxide serves as a potent oxidizing agent in the acidic environment provided by oxalic acid. The final complex is photosensitive; Iron(III) oxalate complexes can undergo photoreduction back to Iron(II), explaining why the compound must be stored in the dark.
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The experimental section is the heart of any chemistry paper, detailing the methodologies used to conduct the research. For students and educators accessing the text digitally,
Each experiment includes specific safety instructions, and hazardous substances have been replaced by less harmful ones wherever possible. The third edition placed a special focus on environmentally friendly experiments, reflecting the growing importance of green chemistry in chemical education. A typical experiment might include prior reading lists, clear purpose statements, and instructions for the safe handling and disposal of materials.
This tripartite structure is one of the book’s most distinctive features. As one reviewer noted, the book “is still the only inorganic laboratory manual that contains separate sections for introductory, intermediate, and advanced experiments,” providing instructors with flexibility in designing courses tailored to students of varying skill levels.
The book has evolved significantly across its three editions, each building on the last to incorporate new science and pedagogical insights. Inorganic Experiments , edited by J
However, the multi-author format has also attracted criticism. One reviewer for CHOICE magazine called the book an “unsuccessful attempt to produce a new, much-needed advanced inorganic laboratory book,” noting that the experimental descriptions are “extremely terse and condensed,” containing only “the barest outline needed to conduct the synthesis, with details of experimental techniques and characterization omitted”. The same reviewer pointed out that references at the end of each experiment are not numbered or linked to the text, nor listed in alphabetical or chronological order, making it difficult to know what information to expect from each reference or where in the experiment it applies. The index was also described as “quite poor, listing mostly names of compounds”.
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